Monolithic Silicas in Separation Science: Concepts, Syntheses, Characterization, Modeling and Applications

Edited by the experts and pioneers in the field, this is the first monograph to cover the topic, containing the must-have information hitherto only scattered among journals.
Clearly divided into sections on preparation, characterization and modeling, and applications, this is essential reading for chemists, chromatographers, analytical chemists, biochemists and biologists.


01 Introduction
Part I PREPARATION.

02 Synthetic Concept, Preparation of Silica Monoliths.

03 Preparation and Properties of Various Monolithic Silica Stationary Phases for RP, HILIC; and Ion Exchange Mode Based on Polymer Coated Materials.

Part II CHARACTERIZATION AND MODELING.

04 Physico-chemical and Chromatographic Characterization.

05 Microscopic Characterization.

06 Structure based modelling of the performance of monolithic supports with variable external porosity.

07 Comparision of Column Performance of Particle Packed and Monolithic Columns for HPLC.

Part III APPLICATIONS.

08 Quantitative structure retention relationships in studies of monolithic material.

09 Performance for basic compounds. Silanol activity.

10 Application of monolithic silica for Quality Control of Drugs.

11 Monolithic Stationary Phases for Fast Ion Chromatography.

12 Monolithic Columns for Chiral Separation.

13 High-Speed and High-Efficiency Separations by Utilizing Monolithic Silica Capillary Columns.

14 Silica Capillaries for on-line and off-line MS Analysis.

15 Silica Monoliths for small scale purification of drug discovery compounds.

16 Monolithic Silica Columns in Mulitdimensional LC-MS for Proteomics and Peptidomics.

17 Silica monoliths for SPE and SPME.


Nobuo Tanaka studied chemistry at Kyoto University, Japan. After his postdocs in the US at the Universities of Pennsylvania, Washington and Northeastern University, he came back to Kyoto, where he is Professor at the Institute of Technology. His research interests include development of chromatographic columns and stationary phases, separation of isotopes, isomers and environmental contaminants on solid surfaces. He is editor of Wileys Journal of Separation Science as well as others. He received several awards as the Environmental Award (1994), Award from the Society for Chromatographic Sciences (1998), the Jubilee Silver Medal of the UK Chromatographic Society (2002) and the Japan Society for Analytical Chemistry Award (2004).

Klaus K. Unger started his research career at the Technical University of Darmstadt, Germany, before he moved to the University of Mainz, Germany. He is one of the pioneers in the development of silica based materials for HPLC. He published many scientific papers as well as successful books.

Egidijus Machtejevas is postdoc in the research group of Klaus K. Unger and co-authored already many research papers.

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